Intergranular Corrosion Test (IGC) per ASTM A At TCR Engineering Services, several methods exist for the testing of intergranular corrosion. To conduct. Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels. ASTM A is the specification which governs five practices used to determine if the. Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the.
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Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion. For alloys not listed in this standard, it adtm be necessary to carry out some tests on material in various conditions to determine the threshold. Some suggested criteria for the listed alloys are shown in Table 2, below.
For example, in highly oxidizing solutions, intergranular attack can occur due to intermetallic phases, while attack of carbides may occur somewhat less oxidizing solutions. The weight loss is calculated after each step, xstm reveals if the sample has been properly heat-treated. Contact us by Phone or Email to find out how we can help your industry.
In everyday applications, corrosion varies by materials and solutions. Practice A, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they are not a622 to intergranular attack sensitization.
For an alloy that is not listed, look for an alloy with a similar composition to a listed alloy to determine the most suitable test. At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established corrosion rate for that specific material type. Practice B, also known as the Streicher test, uses weight loss analysis to provide a quantitative measure of the materials performance. This test is used exclusively to determine corrosion in areas high in chromium carbide formations, and is not as effective for intergranular attack caused by other means.
Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.
Please share this page: Classification of structure then provides either acceptance or further testing required, which typically moves you to one of the next practices. This specification is for detecting susceptibility to intergranular attack IGA. ASTM A is a common intergranular corrosion testing method that can quickly screen batches of material to determine corrosion susceptibility.
See Appendix X1 for information regarding test selection.
Work Item s – proposed revisions of this standard. More suitable alternatives are offered in Table 5, below. Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice.
The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as sigma phase, and is also used for materials in strongly oxidizing environments such as nitric acid.
ASTM A Testing: An Overview of Intergranular Corrosion | Element
Samples may be rectangular or cylindrical to suit the test vessel, but where a bend test is required, it is suggested that the sample be a minimum of mm long. ISO is the most rigorous in terms of defining test s262, and says which alloys should use which test methods as follows:. A22 G28 does not require samples to be heat treated.
Good material should have a corrosion rate substantially less than the threshold value. A recent publication on intergranular corrosion. Classification of the structure after A Practice A analysis will determine if the material is acceptable or if additional testing is required.
A bend test followed by a visual or micro-examination s262 used to determine “Pass” or “Fail” of test specimens. From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment.
Intergranular Corrosion Testing: An Overview of ASTM A262
Share on Tumblr Print. Where a standard is included in a purchase specification, this must be followed, although q262 is advised that unsuitable tests, such as the Huey test for duplex and super austenitic stainless steels, are queried. Typical examination magnification is X to X. Link to Active This link will always route to the current Active version of the standard.
Strauss test specimens are boiled in a Astk Sulfate – Sulfuric Acid mixture for 15 hours. Please refer to the specification for more details. In SEM analysis, intergranular corrosion is clear by the dark lines where the grain boundaries are eaten away.
Based on your materials, application, and requirements, the other 4 methods provide specific focuses. Similar to the Streicher test, the Huey adtm method uses a nitric acid solution and subjects the specimen to five hour boiling intervals.
Intergranular simply means that the corrosion is taking place between the grains or crystals, which is where sigma phase or chromium carbides are going to form which makes the material susceptible to IGA.
Metals like stainless steels and aluminum contain elements such as niobium and chromium, often integrated because of their natural corrosion resistance.